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2,6-Diiodo-4-methylphenol

By Thomas Allen,2014-07-30 16:38
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19 3. Experimental 2,6-Diiodo-4-methyl-phenol (2) [5] A solution of iodine (4.71 g, 18.6 mmol, 2.01 eq) and potassium iodide (12.5 g, 75.4 mmol, 8.15 eq) in water (60 ml) was added to a two-phase mixture of p-cresol (1.02 g, 9.25 mmol, 1.00 eq) in CH 2 Cl 2 (80 ml) and potassium carbonate (1.41 g, 10.1 mmol, 1.09 eq) in water (100 ml). T..
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